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响应面法优化沙苑子中黄酮类化合物超声辅助提取工艺

张清安 范学辉 张志琪

食品工业科技2012,Vol.33Issue(19):275-278,334,5.
食品工业科技2012,Vol.33Issue(19):275-278,334,5.

响应面法优化沙苑子中黄酮类化合物超声辅助提取工艺

Ultrasound-assisted extraction technology for flavones from Semen Astragali Complanati optimized by response surface methodology

张清安 1范学辉 2张志琪3

作者信息

  • 1. 陕西师范大学食品工程与营养科学学院,陕西西安710062
  • 2. 陕西师范大学体育学院,陕西西安710062
  • 3. 陕西师范大学化学化工学院.陕西西安710062
  • 折叠

摘要

Abstract

In order to obtain the optimum extraction conditions for flavoness from Semen Astragali Complanati,on the basis of one-factor experiment,the ratio of solvent-to-sample,ultrasonic extraction temperature,particle size and ultrasonic extraction time were optimized by response surface methodology(RSM)and the absorption of extracts for flavones was chosen as the response.The results showed as follows:the maximum absorbance wavelength for the flavones extracts was 323nm,the suitable extractant was 60% acetone,the particle size was 120 mesh,the ultrasonic extraction temperature was 50℃,the ultrasonic extraction time was 60min,and the ratio of solvent-to-sample was 40:1(mL/g).Under these conditions,the crude yield was 16.19%.The morphology for the particles was studied by scanned electron microscopy,many honey-combed microstructures appeared,and hence facilitated the mass transfer and promoted extraction efficiency.

关键词

响应面法/超声/提取/沙苑子/黄酮

Key words

response surface methodology/ultrasound/extraction/Semen Astragali Complanati/flavones

分类

轻工纺织

引用本文复制引用

张清安,范学辉,张志琪..响应面法优化沙苑子中黄酮类化合物超声辅助提取工艺[J].食品工业科技,2012,33(19):275-278,334,5.

基金项目

国家自然科学基金资助项目 ()

陕西省自然科学基金资助项目 ()

中央高校基本科研业务费专项资金资助项目 ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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