响应面法优化超声波辅助提取仿栗籽油工艺及其脂肪酸组成分析OA北大核心CSCDCSTPCD
Response Surface Optimization of Ultrasonic-Assisted Extraction and Fatty Acid Composition Analysis of Sloanea hemsleyana Seed Oil
采用超声波辅助提取仿栗籽油,通过单因素试验和响应面法（RSM）对提取工艺进行优化,并利用气相色谱-质谱联用法测定仿栗籽油的脂肪酸组成。结果表明,超声波辅助提取仿栗籽油的优化工艺条件为以环己烷为提取溶剂、超声工作/间歇时间为3s/1s、超声功率540W、超声时间18min、提取温度60℃、液料比8.6：1（g/mL）,在此工艺条件下,仿栗籽油提取率可达94.53%。气相色谱-质谱联用测定结果表明仿栗籽油中富含不饱和脂肪酸,总含量达到70.13%,其…查看全部>>
Response surface methodology （RSM） was employed to optimize the ultrasound-assisted extraction of essential oil from Sloanea hemsleyana seeds. Meanwhile, the chemical composition of the extracted essential oil was analyzed by GC-MS. The results showed that the optimal extraction conditions were cyclohexane as the best extraction solvent, single ultrasonic treatment for 3 s at a power level of 540 W followed by a 1-s interval, 18 rain of total extraction time…查看全部>>
麻成金;黄伟;黄群;吴竹青;吴丽雅
吉首大学林产化工工程湖南省重点实验室,湖南张家界427000 吉首大学食品科学研究所,湖南吉首416000吉首大学食品科学研究所,湖南吉首416000吉首大学食品科学研究所,湖南吉首416000吉首大学食品科学研究所,湖南吉首416000吉首大学食品科学研究所,湖南吉首416000
轻工纺织
仿栗籽油超声波辅助提取响应面分析气相色谱-质谱联用分析脂肪酸组成
Sloanea hemsleyana seed oilultrasonic-assisted extractionresponse surface analysisGC-MSfatty acid composition
《食品科学》 2012 (16)
24-29,6
湖南省高校创新平台开放基金项目（09K089）林产化工工程湖南省重点实验室开放项目（JDZ201101）
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