食品科学2012,Vol.33Issue(16):35-39,5.
响应面法优化脐橙渣中类柠檬苦素的提取工艺
Optimization of Extraction Process for Limonoids from Navel Orange Residues by Response Surface Methodology
摘要
Abstract
An ultrasonic-assisted method to extract limonoids from navel orange residues left over from juicing using ethanol as the extraction solvent was proposed and optimized. Ethanol concentration, ultrasonic treatment time and extraction tempera- ture were identified as main parameters that influence limonoids yield using Plackett-Burman design combined with the steepest ascent method. A regression equation reflecting the relationship between limonoids yield and these main affecting parameters was established based on Box-Behnken experimental design to optimize the three extraction parameters using response surface methodology. The optimal ethanol concentration, ultrasonic treatment time and extraction temperature were 82%, 18 min and 60 ℃, respectively. Under these conditions, the actual extraction yield of limonoids was 1.632‰, which was close to the predicted value of 1.651‰.关键词
脐橙渣/类柠檬苦素/提取/响应面法/优化Key words
navel orange residue/limonoids/extraction/response surface methodology/optimization分类
轻工纺织引用本文复制引用
吴笑臣,王科军,钟金莲,罗序中..响应面法优化脐橙渣中类柠檬苦素的提取工艺[J].食品科学,2012,33(16):35-39,5.基金项目
江西省科技厅科技支撑计划项目 ()
江西省教育厅科学技术研究项目 ()
江西省教育厅青年科学基金项目 ()
赣州市果业基金项目 ()
赣南师范学院自然科学研究课题 ()