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气相色谱-质谱联用分析杜鹃红山茶挥发性成分

李辛雷 孙振元 李纪元 范正琪 殷恒福

食品科学2012,Vol.33Issue(16):130-136,7.
食品科学2012,Vol.33Issue(16):130-136,7.

气相色谱-质谱联用分析杜鹃红山茶挥发性成分

GC-MS Analysis of Volatile Components in Camellia azalea Flowers

李辛雷 1孙振元 2李纪元 3范正琪 3殷恒福3

作者信息

  • 1. 中国林业科学研究院亚热带林业研究所,浙江富阳311400 中国林业科学研究院林业研究所,林木遗传育种国家重点实验室,北京100091
  • 2. 中国林业科学研究院林业研究所,林木遗传育种国家重点实验室,北京100091
  • 3. 中国林业科学研究院亚热带林业研究所,浙江富阳311400
  • 折叠

摘要

Abstract

Volatile compounds in Camellia azalea flowers at different stages during flower development, in their different parts and at different hours of a day were analyzed by solid phase micro-extraction and gas chromatography-mass spectrometry (GC- MS). Totally 8, 20, 21 and 17 volatile compounds were identified in early-stage, full bloom and withering flowers, respectively. Volatile compounds were released mainly during the early flowering and full bloom stages. During flower development, the content of alcohols revealed a gradual increase. Alkenes, esters and alkanes revealed an initial increase and a final decrease, while aldehydes and ketones revealed a decrease trend during the whole process. Totally 20 compounds were identified in sepals, 22 in petals, 21 in stamens and 13 in pistils. The major parts releasing volatile components were petals and stamens. Alkanes were the most dominant volatile compounds in sepals, stamens and petals, accounting for 49.86%, 51.59% and 44.66% of the total volatiles, respectively, while the most dominant volatile compounds in pistils were aldehydes and ketones with a relative content of 83.87%. An obvious intraday variation was observed in the relative contents of volatile compounds in Camellia azalea flowers. The peak hours for releasing alkenes, alcohols, esters and alkanes were 8:00 to 12:00, while higher release levels of aldehydes and ketones were found from 14:00 to 18:00.

关键词

杜鹃红山茶/挥发性成分/气相色谱-质谱联用法

Key words

Camellia azalea/volatile component/gas chromatography-mass spectrometry (GC-MS)

分类

轻工纺织

引用本文复制引用

李辛雷,孙振元,李纪元,范正琪,殷恒福..气相色谱-质谱联用分析杜鹃红山茶挥发性成分[J].食品科学,2012,33(16):130-136,7.

基金项目

国家自然科学基金青年科学基金项目 ()

浙江省科技计划项目 ()

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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