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荔枝皮原花青素低聚体的定性分析

周玮婧 隋勇 孙智达 谢笔钧

食品科学2012,Vol.33Issue(17):40-43,4.
食品科学2012,Vol.33Issue(17):40-43,4.

荔枝皮原花青素低聚体的定性分析

Qualitative Analysis of Oligomeric Procyanidins from Litchi chinensis Pericarp

周玮婧 1隋勇 2孙智达 2谢笔钧2

作者信息

  • 1. 武汉市食品药品检验所,湖北武汉430012 华中农业大学食品科学技术学院,湖北武汉430070
  • 2. 华中农业大学食品科学技术学院,湖北武汉430070
  • 折叠

摘要

Abstract

Litchi (Litchi chinensis Sonn.) is a subtropical fruit of high commercial value; however, its pericarp results in a reduced market value. In the present study, oligomeric procyanidins from Litchi chinensis pericarp (LPOPC) were prepared and qualitatively analyzed. LPOPC were extracted with ethanol aqueous solution, purified by AB-8 macroporous resin chromatography, and fractionated by Toyopearl HW-40S resin chromatography to obtain LPOPC. LPOPC was found to comprise three fractions with different degrees of polymerization (DP). The results of FT-IR, HPLC and LC-MS analyses revealed that the major components of LPOPC were (-)-epicatechin, procyanidin A2, procyanidin A3. Highly pure monomer, dimmers and trimers were obtained through selective collection of fractions.

关键词

荔枝皮/原花青素/低聚体/LC-MS

Key words

Litchi chinensis pericarp/procyanidins/oligomer/LC-MS

分类

轻工纺织

引用本文复制引用

周玮婧,隋勇,孙智达,谢笔钧..荔枝皮原花青素低聚体的定性分析[J].食品科学,2012,33(17):40-43,4.

基金项目

国家自然科学基金一广东省联合基金项 ()

“十‘五”国家科技支撑计划项目 ()

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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