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多糖组分色谱指纹图谱聚类分析可可粉的掺假鉴别

胡明华 王琴 戴军 陈尚卫 朱松

食品与发酵工业2012,Vol.38Issue(8):173-177,5.
食品与发酵工业2012,Vol.38Issue(8):173-177,5.

多糖组分色谱指纹图谱聚类分析可可粉的掺假鉴别

Adulteration Detection of Cocoa Powder by Clustering Analysis of Polysaccharide Components

胡明华 1王琴 2戴军 1陈尚卫 1朱松1

作者信息

  • 1. 江南大学食品科学与技术国家重点实验室,江苏无锡214122
  • 2. 无锡市产品质量监督检验所,江苏无锡214101
  • 折叠

摘要

Abstract

In order to establish cocoa adulterhting detection methods, polysaccharide contained in cocoa powder was extracted by Ultrasound assisted method, then hydrolyzed with sulfuric acid solution, and finally derivatized with 1- phenyl-3 - methyl -5 - pyrazolone (PMP) to get cocoa polysaccharide fingerprints by high performance liquid chromatography (HPLC). According to the relative peaks areas of the common peaks, adulteration detection of cocoa powder was attempted successfully by system clustering analysis (HCA) method. The results showed that cocoa powder adulterated with more than 15% cocoa shell could be identified by this method.

关键词

可可粉/掺假检测/高效液相色谱法/聚类分析

Key words

Cocoa powder/adulteration detection/high performance liquid chromatography/clustering analysis

分类

轻工纺织

引用本文复制引用

胡明华,王琴,戴军,陈尚卫,朱松..多糖组分色谱指纹图谱聚类分析可可粉的掺假鉴别[J].食品与发酵工业,2012,38(8):173-177,5.

基金项目

江苏省质量技术监督局科技项目 ()

食品与发酵工业

OA北大核心CSCDCSTPCD

0253-990X

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