中国食物与营养2012，Vol.18Issue(10)：51-53,3.
SPE-GC/MS外标法测定酒中氨基甲酸乙酯
Determination of Ethyl Carbamate in Wine by SPE-GC/MS with External Standard Method
李拥军1
作者信息
- 1. 甘肃省疾病预防控制中心,兰州730000
- 折叠
摘要
Abstract
The study established a method for determination of ethyl earbamate in wine by solid phase extraction (SPE) and gas chro- matograph-mass spectrometry (GC/MS) . The samples were extracted by the SPE little diatomite column, then washed with ethyl acetate/ ether elution. Determination and confirmation were performed by GC/MS at selective ionsmonitoringmode with external standard method. The calibration curve showed a good linear relationship in the range of 10--120μg,/L, and the correlation coefficient r2 was 0. 9993, The lowest concentration determined was 1.6μg/kg, and quantitative limits was 3.0μg/kg. The extraction recovery was 81.0%--97.4% , and the RSD was 2. 6% --5.5% (n = 6) . The method was sensitive, accurate and could be used for determination of ethyl carbamate in wine.关键词
固相萃取-气相色谱-质谱（SPE-GC/MS）/外标法/氨基甲酸乙酯/酒Key words
SPE-GC-MS/external standard method/ethyl carbamate/wine分类
轻工纺织引用本文复制引用
李拥军..SPE-GC/MS外标法测定酒中氨基甲酸乙酯[J].中国食物与营养,2012,18(10):51-53,3.
