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离子沉淀法分离连翘槲皮素的工艺条件

欧阳玉祝 魏燕 张曦 旷超阳 梁明

食品科学2012,Vol.33Issue(20):38-41,4.
食品科学2012,Vol.33Issue(20):38-41,4.

离子沉淀法分离连翘槲皮素的工艺条件

Optimization of Ion Precipitation Conditions for Separation of Quercetin from Fructus Forsythiae

欧阳玉祝 1魏燕 1张曦 2旷超阳 1梁明1

作者信息

  • 1. 吉首大学食品科学研究所,湖南 吉首 416000
  • 2. 湖南省怀化市质量监督局,湖南 怀化 418000
  • 折叠

摘要

Abstract

In order to develop a method for the separation of quercetin from ethanol extract from Fructus Forsythiae, the effects of precipitant dose, temperature and stirring time on quercetin yield were explored. The final product was analyzed by HPLC using quercetin standard. The results showed that the adding 0.60 g of sodium carbonate and 1.00 g of zinc acetate and stirring for 40 min provided a quercetin yield of 4.20% from the 60% ethanol extract from 4.00 g of Fructus Forsythiae. The resulting precipitate showed an HPLC profile similar to that of quercetin standard.

关键词

连翘/槲皮素/锌离子沉淀法/分离

Key words

Fructus Forsythiae/quercetin/zinc ion precipitation method/separation

分类

轻工纺织

引用本文复制引用

欧阳玉祝,魏燕,张曦,旷超阳,梁明..离子沉淀法分离连翘槲皮素的工艺条件[J].食品科学,2012,33(20):38-41,4.

基金项目

湖南省科技厅科技计划项目(2008FJ3077) (2008FJ3077)

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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