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玉米油脱臭馏出物固体酸催化的甲酯化反应条件优化

杨铭铎 张美杨 曲彤旭 王媛 王耀晖

包装与食品机械2012,Vol.30Issue(6):1-5,5.
包装与食品机械2012,Vol.30Issue(6):1-5,5.DOI:10.3969/j.issn.1005-1295.2012.06.001

玉米油脱臭馏出物固体酸催化的甲酯化反应条件优化

Esterification Treatment of Maize Germ Oil Deodorized Distillate by Solid Acid Catalysis

杨铭铎 1张美杨 2曲彤旭 3王媛 1王耀晖2

作者信息

  • 1. 哈尔滨商业大学中式快餐研究发展中心博士后科研基地,哈尔滨150076
  • 2. 哈尔滨商业大学食品工程学院,哈尔滨150076
  • 3. 黑龙江省普通高校食品科学与工程重点实验室,哈尔滨150076
  • 折叠

摘要

Abstract

The article carried out a series of experiments about methyl esterification of fatty acid in deodorizer distillate, which was catalyzed by the strongly-acidic cationic exchange resin. The resins were selected, pre-treated and dried. NKC-9 resin was chosen as the catalyst. The single factor is undertaken in order to get the optimal combination parameters. The process is optimized for the esterification of maize germ oil deodorizer distillate with methanol under following conditions: methanol: MGODD is 2:1 , catalyzed by NKC-9 resin at 60t for 5h. The results showed that strongly-acidic cationic exchange resin had perfect effect on catalyzing methyl esterification of fatty acid in deodorizer distillate;esterification rate was up to 97. 8%.

关键词

甲酯化/脂肪酸/强酸性阳离子交换树脂/酯化率

Key words

methyl esterification/ fatty acid/ strongly-acidic cationic resin/ esterification rate

分类

轻工纺织

引用本文复制引用

杨铭铎,张美杨,曲彤旭,王媛,王耀晖..玉米油脱臭馏出物固体酸催化的甲酯化反应条件优化[J].包装与食品机械,2012,30(6):1-5,5.

基金项目

国家人事部留学回国人员科技活动择优资助项目(200306AD) (200306AD)

包装与食品机械

OACSTPCD

1005-1295

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