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酒醅发酵过程中氨基甲酸乙酯与尿素的变化

范文来 徐岩 史斌斌

食品工业科技2012,Vol.33Issue(23):171-174,4.
食品工业科技2012,Vol.33Issue(23):171-174,4.

酒醅发酵过程中氨基甲酸乙酯与尿素的变化

Evolvement of ethyl carbamate and urea from fermented grains in the fermentation process of Chinese liquor

范文来 1徐岩 1史斌斌1

作者信息

  • 1. 教育部工业生物技术重点实验室,江南大学生物工程学院,酿造微生物与应用酶学研究室,江苏无锡214122
  • 折叠

摘要

Abstract

The quantitative method of ethyl carbamate (EC)of daqu and fermented grains was established. EC of samples were isolated with ultrapure water under an ultrasound cleaning bath, and extracted with headspace solid -phase microextraction( HS- SPME), and detected and identified by gas chromatography- mass spectrometry (GC-MS).The colorimetric method was employed for determining of urea of solid state matrix.The results showed that the changes of EC and urea levels of fermented grains were similar in various aroma type liquors.And the urea increased,and EC also increased with fermentation time.The concentration of EC of fermented grains was range from 110-130μg/kg,and the concentration of urea was 26-80mg/kg.

关键词

白酒大曲和酒醅/氨基甲酸乙酯/尿素/顶空固相微萃取/气相色谱-质谱

Key words

daqu and fermenting grains of Chinese liquors/ethyl carbamate (EC)/urea/headspace solid- phase microextraction ( HS- SPME)/gas chromatographymass spectrometry ( GC- MS )

分类

轻工纺织

引用本文复制引用

范文来,徐岩,史斌斌..酒醅发酵过程中氨基甲酸乙酯与尿素的变化[J].食品工业科技,2012,33(23):171-174,4.

基金项目

十二五国家科技支撑计划(2012BAK17811). ()

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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