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不同前处理方法对蔬菜中有机磷农药残留检测的影响

田憬若 陈文 张长江 孙惜时 谈甜甜 任娇

现代食品科技2013,Vol.29Issue(3):664-667,4.
现代食品科技2013,Vol.29Issue(3):664-667,4.

不同前处理方法对蔬菜中有机磷农药残留检测的影响

Effect of Different Pre-treatment Methods on Detection Results of Organophosphorus Pesticide Residue Vegetables

田憬若 1陈文 1张长江 1孙惜时 1谈甜甜 1任娇1

作者信息

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摘要

Abstract

To improve pre-treatment methods in vegetables organophosphorus pesticide residue detection, GB method, oscillation extraction method and ultrasonic extraction have been used to extract the pesticide residue in vegetables; And then enzyme inhibition method was used to determine the effect of ultrasonic time and the affects of three different ways (direct measurement, active carbon adsorption after filtration and 0.45 μm film filtration) were compared. The best pre-treatment methods was ultrasonic extracting for 10 min followed by a 0.45 μm film filtration, with which the response rate was the highest. Compared with the GB method, the accuracy, recovery and reproducibility of this method were higher.

关键词

蔬菜/有机磷农药/前处理/酶抑制法

Key words

vegetables/ organophosphorus pesticide/ pre-treatment/ enzyme Inhibition

引用本文复制引用

田憬若,陈文,张长江,孙惜时,谈甜甜,任娇..不同前处理方法对蔬菜中有机磷农药残留检测的影响[J].现代食品科技,2013,29(3):664-667,4.

现代食品科技

OA北大核心CSTPCD

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