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离子色谱法测定酒中的有机酸和无机阴离子

潘丙珍 刘青 庞世琦 张斯 李志勇 李荀 陈文锐

现代食品科技2013,Vol.29Issue(4):876-880,902,6.
现代食品科技2013,Vol.29Issue(4):876-880,902,6.

离子色谱法测定酒中的有机酸和无机阴离子

Determination of Organic Acids and Mineral Anions in Liquor by Ion Chromatography

潘丙珍 1刘青 1庞世琦 1张斯 1李志勇 1李荀 1陈文锐1

作者信息

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摘要

Abstract

A new method was established to determine organic acids and mineral anions in liquor by ion chromatography with conducting detection. The samples were diluted by water and filtrated with 0.45 um membrane. The samples solution were injected and analysized. Ionpac ASH was selected as the separation column. The gradient KOH solution with a flow rate 1.0 mL/min was used as eluent. Auto-generated conducting detection ASRS-4mm was used. The method had good relativity (the correlative coefficients(r) were 0.9909-0.9997). and the extraction recoveries were 81.0-117.8%. In addition, the RSD were less than 5.0%. and the detection limits were 0.015-0.152 mg/L. The method had a wide linear range, good repeatability and accuracy.

关键词

离子色谱/电导检测//有机酸/无机阴离子

Key words

ion chromatography/ conductivity detection/liquor/ organic acids/mineral anions

引用本文复制引用

潘丙珍,刘青,庞世琦,张斯,李志勇,李荀,陈文锐..离子色谱法测定酒中的有机酸和无机阴离子[J].现代食品科技,2013,29(4):876-880,902,6.

基金项目

广东省科技计划项目(2011B050400025),质检公益性行业科研专项(201210104-2),广东省科技计划项目(2010B020316006) (2011B050400025)

现代食品科技

OA北大核心CSTPCD

1673-9078

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