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不同前处理对原子荧光法测定海产品总砷的影响

马国军

中国食品添加剂Issue(3):238-241,4.
中国食品添加剂Issue(3):238-241,4.

不同前处理对原子荧光法测定海产品总砷的影响

Study on the influence of pretreatments in total arsenic determination in seafood by atomic fluorescence spectrometer

马国军1

作者信息

  • 1. 杭州市萧山区质量计量监测中心,杭州311215
  • 折叠

摘要

Abstract

The influences of microwave digestion,dry ashing,wet digestion and microwave-wet digestion pre-treatments on determination of total arsenic in seafood by hydride generation atomic fluorescence were studied.Results show that different pretreatment has a great influence on the results of total arsenic:microwave digestion is not suitable for the total arsenic in seafood,dry ash pretreatment solution does not work well in sea weeds plant seafood ; nitric acid-perchloric acid-sulfuric acid wet digestion and microwave-wet digestion (with perchloric acid,sulphuric acid) can be used as pretreatments of seafood.The recycling rate of the two methods are more than 90%

关键词

前处理/原子荧光/总砷/海产品

Key words

pretreatment / atomic fluorescence spectrometry/ total arsenic / seafood

分类

轻工纺织

引用本文复制引用

马国军..不同前处理对原子荧光法测定海产品总砷的影响[J].中国食品添加剂,2013,(3):238-241,4.

中国食品添加剂

OA北大核心CSTPCD

1006-2513

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