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离子交换树脂对马尾松松针中草酸的分离纯化

陈英 刘成国

食品工业科技2013,Vol.34Issue(15):119-123,5.
食品工业科技2013,Vol.34Issue(15):119-123,5.

离子交换树脂对马尾松松针中草酸的分离纯化

Separation and purification of shikimic acid from pine needles with ion exchange resin

陈英 1刘成国1

作者信息

  • 1. 湖南农业大学食品科学技术学院,湖南长沙410128
  • 折叠

摘要

Abstract

The adsorption and desorption rates of 4 types of adsorption resins towards shikimic acid from the Pine Needles were investigated.Among the studied ion exchange resin,331 anion exchange resin was the most suitable to purify crude shikimic acid from the Pine Needles.When 4BV of 1.5mg/mL sample was flowed through 331 anion exchange resin column at a speed of 2mL/min,the adsorption of the 331 anion exchange resin reached dynamic equilibrium.The adsorbed shikimic acid could be completely eluted with 8BV of 2% sodium hydroxide solution at 4mL/min.After the purification,the purity of shikimic acid was increased from 25% to 90%,resulting in a purification yield of 90.9%.

关键词

离子交换树脂/331弱碱性阴离子交换树脂/莽草酸

Key words

ion exchange resin/331 weakly basic anion exchange resin/shikimic acid

分类

轻工纺织

引用本文复制引用

陈英,刘成国..离子交换树脂对马尾松松针中草酸的分离纯化[J].食品工业科技,2013,34(15):119-123,5.

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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