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碳-4植物糖超标蜂蜜样品的多维分析

罗海英 罗东辉 冼燕萍 侯向昶 郭新东 吴玉銮 董浩

现代食品科技2013,Vol.29Issue(8):1989-1993,1988,6.
现代食品科技2013,Vol.29Issue(8):1989-1993,1988,6.

碳-4植物糖超标蜂蜜样品的多维分析

Multidimensional Analysis of Honey Samples with Excessive Amounts of C-4 Plant Sugar

罗海英 1罗东辉 1冼燕萍 1侯向昶 1郭新东 1吴玉銮 1董浩1

作者信息

  • 1. 广州市质量监督检验研究院,国家加工食品质量监督检验中心(广州),广州市食品安全检测技术重点实验室,广州市食品安全风险动态监测与预警研究中心,广东广州510110
  • 折叠

摘要

Abstract

In this paper,21 honey samples with excessive amounts of C-4 plant sugar were chosen from 120 specimens obtained from food market.Element analyzer-isotope ratio mass spectrometry (EA-IRMS),liquid chromatography-isotope ratio mass spectrometry (LC-IRMS)and liquid chromatography (LC) were adopted to detect the δ13C values and the amount of C-4 plant sugar.The results indicated that the honey samples with excessive amounts of C-4 plant sugar still occupy a certain proportion in food market and the over-standard rate of this batch was 16.94%.Several samples were detected with serious excessive C-4 plant sugar,one of which haDs the highest amount of 82.35%.The honey samples with excessive C-4 plant sugar can be summarized as the following three categories.(1) Samples with slightly excessive C-4 plant sugar:the standard-exceeding rate of those samples was 7~10%,and their △δ13CF-G and △δ13Cmax values were not far from the requirements of the real honey.(2) Samples adulterated with starch products of C-4 plant source:these samples had a high amount of oligosaccharide and larger △δ13Cmmax (3) Samples adulterated with high fructose com syrup; no oligosaccharide was found in these samples and their δ13CF and δ13CG completely lost the characteristics of C-3 plant.

关键词

蜂蜜/碳-4植物糖/掺假/同位素比值质谱

Key words

honey/ C-4 plant sugar/ adulteration/ isotope ratio mass spectrometry (IRMS)

引用本文复制引用

罗海英,罗东辉,冼燕萍,侯向昶,郭新东,吴玉銮,董浩..碳-4植物糖超标蜂蜜样品的多维分析[J].现代食品科技,2013,29(8):1989-1993,1988,6.

基金项目

广州市科技计划项目(2011J2200016 ()

[2011]233-34) ()

广东省质量技术监督局科技项目(2011ZS01) (2011ZS01)

现代食品科技

OA北大核心CSTPCD

1673-9078

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