中国食品添加剂Issue(4)：174-178,5.
超临界流体强制分散溶液技术制备叶黄素超细微粒
Preparation of lutein microparticle via solution enhanced dispersion by supercritical fluids technology
摘要
Abstract
The micronization of natural lutein was carried out using dichloromethane as solvent and carbon dioxide as antisolvent via the Solution Enhanced Dispersion by Supercritical Fluids (SEDS) technology.The nubbly lutein crystals of 50μm diameters were successfully micronized by the SEDS process to rod-like or twisted fiber-like microparticles with 3 ～ 20μm diameters.Morphologies and particle sizes (PSs) of lutein microparticles were analyzed by the scanning electron microscopy and optical microscopy.The influences of operating variables include initial solution concentration and flow rate,pressure and temperature on PSs and morphologies of the lutein microparticles obtained by the SEDS-PA process were discussed.The results shown that the effects of temperature,initial solution concentration and flow rate on PS of the lutein microparticles were more significant,while the pressure had little effects on PSs.关键词
叶黄素/超临界流体/SEDS/超细微粒Key words
lutein/ supercritical fluid/ SEDS/ microparticle分类
轻工纺织引用本文复制引用
贾慧劼,洪海龙,索全伶,韩利民,竺宁..超临界流体强制分散溶液技术制备叶黄素超细微粒[J].中国食品添加剂,2013,(4):174-178,5.基金项目
内蒙古自治区自然科学基金项目(2010BS0204) （2010BS0204）
内蒙古自治区高等学校科学研究项目(NJZZ12048) （NJZZ12048）
内蒙古工业大学科学研究项目(ZD200904,ZS201016). （ZD200904,ZS201016）
