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微波萃取-高效液相色谱法测定食品塑料包装材料中双酚A含量

吴茵琪 钟月香 蒋小良

包装与食品机械Issue(3):62-65,4.
包装与食品机械Issue(3):62-65,4.DOI:10.3969/j.issn.1005-1295.2015.03.015

微波萃取-高效液相色谱法测定食品塑料包装材料中双酚A含量

Determination of Bisphenol A in Food Plastics Packings Materials by Microwave-assisted Extraction-high Performance Liquid Chromatograph

吴茵琪 1钟月香 1蒋小良1

作者信息

  • 1. 江门出入境检验检疫局,广东江门 529000
  • 折叠

摘要

Abstract

A method for the determination of bisphenol A (BPA)in food packing materials was developed by high performance liquid chromatograph (HPLC)with microwave extraction.The optiomized analytical con-dition are as follows:extraction temperature is 80℃,extraction time is 20min,extraction solvent is methanol. Under the optimal condition of determination,the linearity range of the testing method was 0.1 ~20 mg/L,the correlation coefficient was 0.9998,the lowest detection limit was 0.1 mg/kg,the recovery rate and relative standard deviation were 88.9% ~99.6% and less than 2.2 % respectively.

关键词

微波萃取/高效液相色谱法/双酚 A/食品塑料包装材料

Key words

microwave extraction/high performance liquid chromatograph/bisphenol A/food plastics packing materials

分类

轻工纺织

引用本文复制引用

吴茵琪,钟月香,蒋小良..微波萃取-高效液相色谱法测定食品塑料包装材料中双酚A含量[J].包装与食品机械,2015,(3):62-65,4.

基金项目

广东检验检疫局科技计划项目 ()

包装与食品机械

OACSTPCD

1005-1295

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