茶叶科学Issue(2)：145-150,6.
茶叶及茶多糖中氟测定前处理方法的比较研究
Comparison on the Pretreatment Methods of Tea and Tea Polysaccharides for Determination of Fluorine Content
摘要
Abstract
The influence of sample pretreatment methods including boiling water extraction (BWE),acidic solution extraction (ASE) and alkalizing and burning to ash(ABA) on fluorine content in tea and tea polysaccharides was investigated. The results showed that the fluorine contents of tea and tea polysaccharide pretreated with ABA were much higher than that of BWE and ASE method (P<0.01). The fluorine content of tea pretreated with BWE was significantly higher than ASE (P<0.05, P<0.01). The further test on precision and recovery of ABA and fluoride ion selective electrode method was investigated. Results showed that the recovery of fluorine in tea and tea polysaccharide were 91.07%-94.40% and 83.04%-90.32%, respectively, with RSD of 1.44%-2.54% for tea and 0.68%-1.03% for tea polysaccharide, which indicated the result of fluorine determination by this method could represent the real fluorine content in tea and tea polysaccharide with accuracy, reliability and stability. It was also suggested that the ABA and fluoride ion selective electrode method could be more suitable for determination of total fluorine in tea and tea extracts.关键词
茶叶/茶多糖/氟含量/预处理方法/氟离子选择电极法Key words
tea/tea polysaccharide/fluorine content/pretreatment/fluoride ion selective electrode分类
农业科技引用本文复制引用
朱晓静,房峰祥,张月华,倪德江,陈玉琼..茶叶及茶多糖中氟测定前处理方法的比较研究[J].茶叶科学,2015,(2):145-150,6.基金项目
国家自然科学基金项目（31170646/C161104）资助 （）
