中国果菜Issue(12)：22-24,34,4.
LC-MS/MS法测定酒中罂粟壳生物碱
Investigation of Alkaloids of Pericarpium Papaveris in Wines by LC-MS/MS
景赞 1刘超1
作者信息
- 1. 乐山市食品药品检验检测中心，四川乐山614000
- 折叠
摘要
Abstract
To develop a method for alkaloids of pericarpium papaveris (morphine, thebaine, papaverine and narcotine) in distilled wines and mixed wines by LC-MS/MS. The wines were separated in ODS-C18 column with acetonitrile-ammonium acetate solution after purificatied by PCX solid-phase extraction column. The data was quantified by external standard method under the positive ion mode. The limits of detection for morphine, thebaine, papaverine and narcotine were 20ng/mL, 5ng/mL, 5ng/mL and 5ng/mL, the average recoveries between 91.1%~101.4%. This method was accurate and reliable with simple sample prepatation, and could be used for the determination of alkaloids of pericarpium papaveris in wines.关键词
酒/液质联用/罂粟壳生物碱成分Key words
Wines/LC-MS/MS/alkaloids of pericarpium papaveris分类
轻工纺织引用本文复制引用
景赞,刘超..LC-MS/MS法测定酒中罂粟壳生物碱[J].中国果菜,2015,(12):22-24,34,4.
