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橄榄油实际与理论ECN42甘三酯含量绝对差值测定方法研究

张冰 张蕊

粮油食品科技2016,Vol.24Issue(5):77-82,6.
粮油食品科技2016,Vol.24Issue(5):77-82,6.

橄榄油实际与理论ECN42甘三酯含量绝对差值测定方法研究

Research on determination of the difference between actual and theoretical content of triacylglycerols with ECN42 in olive oil

张冰 1张蕊1

作者信息

  • 1. 国家粮食局科学研究院,100037 北京
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摘要

Abstract

The method of calculating theoretical content of triacylglycerols with ECN42 in olive oil was introduced,which distinguished adulteration of olive oil by determination of the absolute difference be-tween actual and theoretical content of triacylglycerols with ECN42(△ECN42). The HPLC condition to quantify ECN42,and the reproducibility of the method was researched. The results showed that using dif-ferential refractometer as the detector,column temperature 38 ℃,mobile phase acetone / acetonitrile (50∶ 50,V/ V),flow rate 1. 5 mL/ min,under the condition,it showed a good chromatographic separation effect with good repeatability,and RSD less than 1% and S R between 0. 02 and 0. 11. It provided basis for instituting national standard.

关键词

橄榄油/掺伪/甘三酯/等效碳数42/△等效碳数42

Key words

olive oil/adulteration/triacylglycerols/ECN42/△ECN42

分类

轻工纺织

引用本文复制引用

张冰,张蕊..橄榄油实际与理论ECN42甘三酯含量绝对差值测定方法研究[J].粮油食品科技,2016,24(5):77-82,6.

粮油食品科技

OACSTPCD

1007-7561

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