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基于中波近红外光谱构建生鲜鸡肉胆固醇定量分析模型

王辉 田寒友 张顺亮 邹昊 刘飞 李文采 李家鹏 陈文华 乔晓玲

食品科学2016,Vol.37Issue(20):134-140,7.
食品科学2016,Vol.37Issue(20):134-140,7.DOI:10.7506/spkx1002-6630-201620022

基于中波近红外光谱构建生鲜鸡肉胆固醇定量分析模型

Establishment of Quantitative Analysis Model of Chicken Cholesterol Based on Medium-Wavelength Near-Infrared Spectroscopy

王辉 1田寒友 1张顺亮 1邹昊 1刘飞 1李文采 1李家鹏 1陈文华 1乔晓玲1

作者信息

  • 1. 中国肉类食品综合研究中心,肉类加工技术北京市重点实验室,北京食品科学研究院,北京 100068
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摘要

Abstract

In this research spectral information for commercially available chicken breast samples was extracted in the medium wavelength region of near-infrared (NIR) and used for establishing a quantitative analysis model of cholesterol concentration using partial least squares (PLS) regression, and the prediction accuracy of the model was analyzed. The modeling was investigated with respect to outlier elimination and optimized combined use of various spectral preprocessing methods. The optimum quantitative analysis model was achieved with two cycles of outlier elimination and the combined use of SG first derivative, SG smoothing and De-trending for spectral preprocessing. The model parameters standard error of calibration (SEC), correlation coefifcient of calibration set (Rc), standard error of prediction (SEP), correlation coefifcient of validation set(Rp), ratio of performance to standard deviate (RPD), relative standard error of prediction (RSEP), the number of principal factors (PF) and SEP/SEC were 4.534 8, 0.919 7, 7.437 5, 0.812 0, 2.844 7, 9.44%, 5, and 1.640 1, respectively. The experimental results showed that the model had better prediction accuracy in test set (P> 0.05), especially in the range of 60–100 mg/100 g, and could be applied to analyze the cholesterol concentration of commercially available fresh chicken and chicken products.

关键词

近红外光谱/中波区/生鲜鸡肉/胆固醇/定量分析

Key words

near-infrared spectroscopy/medium wavelength region/fresh chicken/cholesterol concentration/quantitative analysis

分类

化学化工

引用本文复制引用

王辉,田寒友,张顺亮,邹昊,刘飞,李文采,李家鹏,陈文华,乔晓玲..基于中波近红外光谱构建生鲜鸡肉胆固醇定量分析模型[J].食品科学,2016,37(20):134-140,7.

基金项目

“十二五”国家科技支撑计划项目 ()

食品科学

OA北大核心CSCDCSTPCD

1002-6630

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