食品与机械2016，Vol.32Issue(11)：35-38,4.DOI:10.13652/j.issn.1003-5788.2016.11.008
气相色谱-质谱法测定奶粉中香兰素含量的方法建立
Determination of vanill in and ethyl-vanill in in mi lk powder by gas chromatography-mass spectrometry
摘要
Abstract
A method for determination of vanillin and ethyl-vanillin in milk powder was established by auto headspace solid-phase micro-ex-traction coupled with gas chromatography-mass spectrometry (GC—MS),and the influence factor were also studied,such as solid phase micro-extraction head,time and temperature of adsorption and de-sorption.As a result,the limits of determination (LOD)of vanillin and ethyl-vanillin were 0.5 mg/kg.The spiked recovery was between 90.0% and 100%,and the RSD ranged from 1 .9%~4.1 %(n = 6). This method could eliminate the interference of complicated matrix, conveniently,quickly and exactly,which was applicable for quick de-termination of vanillin and ethyl-vanillin content in milk powder.关键词
香兰素/乙基香兰素/奶粉/气相色谱-质谱Key words
vanillin/ethyl-vanillin/milk powder/GC-MS引用本文复制引用
郑璇,黄瑾,林洁,李菊,韦晓群,蔡纯,陈燕芬,冯婕莉,郭庆园..气相色谱-质谱法测定奶粉中香兰素含量的方法建立[J].食品与机械,2016,32(11):35-38,4.基金项目
国家质检总局科技项目(编号:2015IK065) （编号:2015IK065）
