食品工业科技2017，Vol.38Issue(5)：274-278,5.DOI:10.13386/j.issn1002-0306.2017.05.043
分子蒸馏法纯化宽叶缬草挥发油中的乙酸龙脑酯
Purification of bornyl acetate in volatile oil of valeriana officinalis L.var.latifolia Miq by molecular distillation
摘要
Abstract
Molecular distillation was used for the further purification of the volatile oil from roots of valeriana officinalis L.var.latifolia Miq.The best process parameters,including temperature,feed rate,and scraping rate,of molecular distillation technique for separating the volatile oil were studied by response surface methodology based on single factor experiment.The content was detected by GC under the conditions of elastic quartz capillary column TR-5,detector temperature 250 ℃,gasification temperature 250 ℃,distributary refer 50∶ 1.The optimal extraction processing parameters were material-feeding rate of 82 mL/h,distillation temperature of 68 ℃ and scraping rate of 188 r/min.Under the optimal processing conditions,the quality of volatile oil was markedly improved,and the content of bornyl acetate was 77.46％.The molecular distillation technique that could get the product with higher content of bomyl acetate has a very good prospect in industry.关键词
缬草挥发油/分子蒸馏/乙酸龙脑酯/响应面法Key words
the volatile oil in valeriana officinalis L.var.latifolia Miq/molecular distillation/bornyl acetate/response surface methodology分类
轻工纺织引用本文复制引用
李雄,吕庆银,李岑,吴威,赵伟,张振..分子蒸馏法纯化宽叶缬草挥发油中的乙酸龙脑酯[J].食品工业科技,2017,38(5):274-278,5.基金项目
贵州省科学技术项目(黔科合J字[2011]3004). （黔科合J字[2011]3004）
