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熔融共结晶法制备赤藓糖醇-三氯蔗糖共晶体

王海蓉 张春桃 梁文懂

现代食品科技2017,Vol.33Issue(5):228-232,195,6.
现代食品科技2017,Vol.33Issue(5):228-232,195,6.DOI:10.13982/j.mfst.1673-9078.2017.5.036

熔融共结晶法制备赤藓糖醇-三氯蔗糖共晶体

Co-crystals and Co-crystallization of Meso-erythritol and Sucralose

王海蓉 1张春桃 1梁文懂1

作者信息

  • 1. 武汉科技大学化学工程与技术学院,煤炭转化与新型炭材料湖北省重点实验室,湖北武汉430081
  • 折叠

摘要

Abstract

Co-crystallization technologies have been known as the leading edge in the frne chemicals and pharmaceuticals industries.The melt co-crystallization process was adopted to produce the solid recombination product of meso-Erythritol and sucralose,the structure and properties of which had been characterized and analyzed by using TG-DSC,XRD,and SEM.The results indicated that the solid recombination product of meso-Erythritol and sucralose is a co-crystal.The endothermic peak temperatures of the thermal decomposition of the co-crystals and pristine sucralose were found to be 156.2 ℃ and 134.4 ℃,respectively,indicating co-crystallization enhanced the thermal stability ofsucralose.Seeding load and crystal size distribution (CSD) of the seeds were found to have significant effects on the CSD and bulk density of the co-crystal products of meso-Erythritol and sucralose.When the process parameter of the co-crystallization of meso-Erythritol and sucralose was a seeding load of 10 wt% with CSD of 120~200#,the co-crystal products with 30~60# accounted for 91.8% of the whole product crystals,and its bulk density was 0.82 g/cm3.

关键词

共结晶/共晶体/赤藓糖醇/三氯蔗糖

Key words

co-crystallization/co-crystals/meso-erythritol/sucralose

引用本文复制引用

王海蓉,张春桃,梁文懂..熔融共结晶法制备赤藓糖醇-三氯蔗糖共晶体[J].现代食品科技,2017,33(5):228-232,195,6.

基金项目

湖北省大学生创新创业训练计划项目(201410488034) (201410488034)

现代食品科技

OA北大核心CSTPCD

1673-9078

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