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Plackett-Burman设计及响应面法优化芹菜中总黄酮的超声提取工艺

赵刚 顾佳丽 励建荣

中国食品学报2017,Vol.17Issue(8):147-155,9.
中国食品学报2017,Vol.17Issue(8):147-155,9.DOI:10.16429/j.1009-7848.2017.08.020

Plackett-Burman设计及响应面法优化芹菜中总黄酮的超声提取工艺

Optimization of Ultrasonic Extraction Conditions of Total Flavonoids from Apium Graveolens by Plackett-Burman Design and Response Surface Analysis

赵刚 1顾佳丽 2励建荣1

作者信息

  • 1. 渤海大学化学化工学院 辽宁锦州121013
  • 2. 渤海大学食品科学与工程学院辽宁省食品安全重点实验室生鲜农产品贮藏加工及安全控制技术国家地方联合工程研究中心 辽宁锦州121013
  • 折叠

摘要

Abstract

The key factors affecting extraction rate of total flavonoids compounds were screen out by Plackett-Burman (PB) design on the basis of single-factor experiments.The key factors affecting ultrasonic extraction were ethanol concentration,ultrasonic time,ultrasonic temperature and liquid-solid ratio.Then the center points of the four factors were determined based on steepest ascent design.Finally,the the optimization extraction condition were carried out by using central composite design.The results showed that the optimal extraction conditions were as follows:ethanol concentration 57.41%,ultrasonic time 52.79 min,ultrasonic temperature 66.34 ℃ and liquid-solid ratio 31.69(mL·g-1).Under the optimum conditions,the predicted value of extraction rate is 7.9001 mg·g-1 and its experimental value is 8.051 mg·g-1.This result indicated that it was perfect to optimize of extraction conditions of total flavonoids compounds from apium graveolens by PB design and BB design.

关键词

Plackett Burman设计/响应面分析法/超声提取法/黄酮/芹菜

Key words

Plackett-Burman design/response surface analysis/ultrasonic extraction/flavonoids compounds/apium graveolens

引用本文复制引用

赵刚,顾佳丽,励建荣..Plackett-Burman设计及响应面法优化芹菜中总黄酮的超声提取工艺[J].中国食品学报,2017,17(8):147-155,9.

基金项目

辽宁省高等学校攀登学者支持计划项目 ()

辽宁省高等学校创新团队计划项目 ()

中国食品学报

OA北大核心CSCDCSTPCD

1009-7848

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