食品科学2017,Vol.38Issue(18):87-92,6.DOI:10.7506/spkx1002-6630-201718014
紫斑牡丹籽饼粕单萜苷类成分的分离鉴定
Isolation and Identification of Monoterpene Glucosides from Seed Cake of Paeonia rockii
摘要
Abstract
Objective: To isolate and identify monoterpene glucosides from the seed cake of Paeonia rockii. Methods:Monoterpene glucosides were isolated and purified by successive column chromatographies on silica gel and Sephadex LH-20 and semi-preparative high performance liquid chromatography (semi-pre-HPLC). Spectroscopic methods were used to elucidate their structure. Results: Eight monoterpene glucosides were isolated from the seed cake of Paeonia rockii. They were identified as β-gentiobiosylpaeoniflorin (1), abiflofin (2), oxyalbiflorin (3), 1-O-β-D-glucopyransoyl-paeonisuffron (4), abiflofin R1 (5), paeonifanin (6), 8-O-debenzoyl-albiflorin (7), and mudanpioside F (8). Conclusions: All of these compounds were isolated from the seed cake of P. rockii for the first time in this study. These compounds and their derivatives were of significant interest for drug research and development. The study may provide important evidence supporting the exploitation of the seed cake of P. rockii.关键词
紫斑牡丹/籽饼粕/化学成分/单萜苷类化合物Key words
Paeonia rockii/seed cake/chemical constituents/monoterpene glucosides分类
轻工纺织引用本文复制引用
刘普,许艺凡,刘佩佩,邱赛西,张惠芳,吴珂,邓瑞雪..紫斑牡丹籽饼粕单萜苷类成分的分离鉴定[J].食品科学,2017,38(18):87-92,6.基金项目
国家自然科学基金委员会-河南省人民政府联合基金项目(U1604192 ()
U1404831) ()
河南省重点科技攻关项目(152102110079 ()
162102310202) ()
河南省高等学校重点科研项目(16A210019) (16A210019)