食品工业科技2017,Vol.38Issue(18):242-246,5.DOI:10.13386/j.issn1002-0306.2017.18.046
ICP-OES/ICP-MS法测定罗汉果中46种元素
Determination of 46 elements in Siraitia grosvenorii by ICP-OES/ICP-MS
摘要
Abstract
A method of inductively coupled plasma optical emission spectrometry (ICP-OES)and inductively coupled plasma mass spectrometry (ICP-MS)was established to determine 46 elements in Siraitia grosvenorii.The detection limit of ICP-OES and ICP-MS were in the range of 0.68~18.10 μg/L and 0.001~0.093 μg/L,respectively.The precision of this method was in the range of 0.73% to 6.83%,and thc recovery varied from 88.7% to ll2.1%.The established method was used to determine the corresponding element content in the certified reference material of bush branch and leaf,which was in agreement with the certified values.The results showed that there were rich trace elements in Siraitia grosvenorii,13 of which were more than 2 mg/kg.The method was simple,rapid and accurate and suitable for the determination of multi-elements in Siraitia grosvenorii simultaneously.关键词
罗汉果/ICP-OES/ICP-MS/元素/稀土元素Key words
Siraitia grosvenorii/ICP-OES/ICP-MS/elements/rare earth elements分类
轻工纺织引用本文复制引用
秦愫妮,黄俊杰,全洗强,陶鑫,秦翠芸..ICP-OES/ICP-MS法测定罗汉果中46种元素[J].食品工业科技,2017,38(18):242-246,5.基金项目
中国地质科学院岩溶地质研究所基本科研业务费资助项目(2015013). (2015013)