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响应面法优化石榴叶总酚的亚临界水提取工艺

闫林林 郑光耀 韦朝宽

食品工业科技2017,Vol.38Issue(19):184-190,7.
食品工业科技2017,Vol.38Issue(19):184-190,7.DOI:10.13386/j.issn1002-0306.2017.19.034

响应面法优化石榴叶总酚的亚临界水提取工艺

Optimization of subcritical water extraction for total phenolics from pomegranate (Punica granatum L.) leaves by response surface methodology

闫林林 1郑光耀 1韦朝宽1

作者信息

  • 1. 中国林业科学研究院林产化学工业研究所,国家林业局林产化学工程重点开放性实验室,江苏南京210042
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摘要

Abstract

The aim of this study was to optimize the technology parameters of subcritical water extraction for extracting total phenolics from pomegranate leaves by response surface methodology.On the basis of single-factor experiments,three-factors and three-level response surface methodology was applied to investigate the effects of extraction temperature,extraction time and solvent/solid ratio on the total phenolics contents.The results showed that model regression was significant,and the established regression equation for phenolics contents had an excellent of fit.The optimized extraction temperature was 134 ℃,extracting time was 31 minutes,and solvent/solid ratio was 52∶1 mL/g.Under the optimized conditions,the total phenolics content was 169.24 mg GAE/g,which was consistent with the predictive value of 173.31 mg GAE/g.In addition,the total phenolic content of the optimized extracts was higher than the reflux extraction using aqueous-organic solvent,and the time was shortened.

关键词

石榴叶/总酚/亚临界水提取/响应面法

Key words

pomegranate leaves/total phenolics/subcritical water extraction/response surface methodology

分类

轻工纺织

引用本文复制引用

闫林林,郑光耀,韦朝宽..响应面法优化石榴叶总酚的亚临界水提取工艺[J].食品工业科技,2017,38(19):184-190,7.

基金项目

中国林业科学研究院林产化学工业研究所研究团队建设创新工程项目(LHSXKQ4). (LHSXKQ4)

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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