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HPLC法测定红景天苷含量的不确定度评定

刘长姣 王思琪 王磊 杨柳

中国食品添加剂Issue(11):155-159,5.
中国食品添加剂Issue(11):155-159,5.

HPLC法测定红景天苷含量的不确定度评定

Uncertainty evaluation of Salidroside content determined by HPLC

刘长姣 1王思琪 1王磊 1杨柳1

作者信息

  • 1. 吉林工商学院粮油食品深加工吉林省高校重点实验室,长春130507
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摘要

Abstract

This purpose of this paper is to evaluate the uncertainty of salidroside content in Rhodiola rosea L.determined by HPLC.Mathematical model was established.The uncertainties of factors that affected the accuracy of result were analyzed and calculated.The results showed that the uncertainties of standard curve and sample determination process were the main sources of uncertainty (u (x)).According to JJF1059-2012,the component uncertainties were synthesized and extended.An expanded uncertainty of 0.35ug/kg was obtained at the confidence probability of 95% and coverage factor of 2.The method provides references for the uncertainty evaluation of salidroside content determined by HPLC.

关键词

红景天苷/不确定度/高效液相色谱法

Key words

salidroside/uncertainty/HPLC

分类

轻工纺织

引用本文复制引用

刘长姣,王思琪,王磊,杨柳..HPLC法测定红景天苷含量的不确定度评定[J].中国食品添加剂,2017,(11):155-159,5.

基金项目

吉林省教育厅“十二五”科学技术研究项目(2014439). (2014439)

中国食品添加剂

OACSTPCD

1006-2513

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