中国食品添加剂Issue(12)：210-213,4.
食品中甜蜜素检测不确定度评定
Evaluation of uncertainty for determination of sodium N-cyclohexylsulfamate in food
陈妍 1鲍晓瑾 1朱洪亮 1倪炜华 1陈晨1
作者信息
- 1. 嘉兴市食品药品检验检测院,嘉兴314000
- 折叠
摘要
Abstract
Sodium N-cyclohexylsulfamate has been used as additives in food production,edible drinks or other food which exceeded the statutory limit,will cause harm to human liver and nervous system,so the detection of sodium cyclamate in food is very important.Due to the existence of measurement errors in the detection process,to improve the accuracy of the detection of sodium N-cyclohexylsulfamate in food,protect food safety effectively.This article was based on JJF1059.1-2012 "measurement uncertainty evaluation and expression" and the new national standard method,GB 5009.97-2016 "determination of sodium N-cyclohexylsulfamate in food ",analyzed and evaluated the uncertainty of Sample weighing,sample volume determination,standard solution preparation and standard work curve fitting during the determination of sodium N-cyclohexylsulfamate in drinks by gas chromatography.When the content of sodium N-cyclohexylsulfamate in the sample was 0.48g/kg,its extended uncertainty was (0.48 + 0.074) g/kg,k=2.The results show that the preparation of standard solution and the stability of GC are the key to the accurate detection of sodium N-cyclohexylsulfamate in food,while the uncertainty of sample weighing and volumetric determination can be neglected.关键词
环己基氨基磺酸钠/气相色谱法/不确定度/饮料Key words
sodium N-cyclohexylsulfamate/gas chromatography/uncertainty/drinks分类
轻工纺织引用本文复制引用
陈妍,鲍晓瑾,朱洪亮,倪炜华,陈晨..食品中甜蜜素检测不确定度评定[J].中国食品添加剂,2017,(12):210-213,4.
