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肉制品中6种人工合成色素的快速测定

蒋荣华 吴玉杰 温和心 龙英全 蔡翔宇 杨昆 江思华 谭春芳

食品工业科技2017,Vol.38Issue(24):278-281,302,5.
食品工业科技2017,Vol.38Issue(24):278-281,302,5.DOI:10.13386/j.issn1002-0306.2017.24.054

肉制品中6种人工合成色素的快速测定

Rapid detection methods for six kinds of synthetic pigments in meat products

蒋荣华 1吴玉杰 2温和心 1龙英全 1蔡翔宇 2杨昆 2江思华 2谭春芳1

作者信息

  • 1. 贵港出入境检验检疫局,广西贵港537100
  • 2. 广西出入境检验检疫局检验检疫技术中心,广西南宁530028
  • 折叠

摘要

Abstract

Objective:To establish a method for simultaneous determination of six kind of synthetic pigments including tartrazine,amaranth,carmine,sunset yellow FCF,allura red and carmosine in meat products by HPLC.Methods:Extracted with ethanol-ammonia-water solution in the samples,then defatted by ether.The pigments were separated on Agilent Poroshell 120 SB-C18 column,by gradient elution with a mobile phases made up of 0.02 mol/L NH4Ac and acetonitrile,determined by diode array detector(DAD).Results:Six kinds of synthetic pigments had good linear relations when the concentration was in the range of 0~ 10 μg/mL and the average recoveries range of 70.33 %~93.08%.The correlation coefficient of regression equations could be up to 0.9999 and relative standard deviation was less than 5 %.Conclusion:The method was simple,quickly,sensitivity and good reproducibility,which could be applicable to determine six kinds of synthetic pigments in meat products for lots of samles superviser detection.

关键词

6种人工合成色素/同时测定/高效液相色谱法/肉制品

Key words

six kinds of synthetic pigments/simultaneous determination/high performance liquid chromatography/meat products

分类

轻工纺织

引用本文复制引用

蒋荣华,吴玉杰,温和心,龙英全,蔡翔宇,杨昆,江思华,谭春芳..肉制品中6种人工合成色素的快速测定[J].食品工业科技,2017,38(24):278-281,302,5.

基金项目

广西畜牧产品中非法添加色素风险评估及检测方法研究与应用(桂科重14121003-4-3). (桂科重14121003-4-3)

食品工业科技

OA北大核心CSCDCSTPCD

1002-0306

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