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FIA-IC法同时测定水中痕量I-、SCN-、ClO4-及草甘膦

刘秋连

食品与机械2017,Vol.33Issue(11):76-79,4.
食品与机械2017,Vol.33Issue(11):76-79,4.

FIA-IC法同时测定水中痕量I-、SCN-、ClO4-及草甘膦

Simultaneous determination of trace amounts of I-, SCN-, ClO4-and Glyphosate in water by FIA-IC

刘秋连1

作者信息

  • 1. 湘潭市食品药品检验所,湖南湘潭411100
  • 折叠

摘要

Abstract

A method to the determination of Iodide,Thiocyanate,Perchlorate and Glyphosate in drinking water by flow injection online preconcentration and Ion chromatography Spectrometry with activated carbon fiber as adsorbent was developed.Using the activated carbon fiber as adsorbent flow injection on-line preconcentration,and by flow injection in the laboratory (FIA)-ion chromatography (IC) combined with technology of adsorption column enrichment of Iodide,Thiocyanate,Perchlorate and Glyphosate were determined.The linear range of the method for trace Iodide,Thiocyanate,Perchlorate and Glyphosate was 0.01 ~5.00 mg/L,the correlation coefficients were 0.997 9,0.999 0.0.998 7 and 0.998 1,and the average recoveries were 94.9% ~99.2 %.

关键词

流动注射/离子色谱/碘离子/硫氰根离子/高氯酸根离子/草甘膦/生活饮用水

Key words

flow injection/chromatography of ions/iodide ion/cyanide ion/perchlorate ion/glyphosate/drinking water

引用本文复制引用

刘秋连..FIA-IC法同时测定水中痕量I-、SCN-、ClO4-及草甘膦[J].食品与机械,2017,33(11):76-79,4.

食品与机械

OA北大核心CSCDCSTPCD

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