食品工业科技2018，Vol.39Issue(8)：221-225,5.DOI:10.13386/j.issn1002-0306.2018.08.040
柱前衍生-高效毛细管电泳法分析不同黄酒的多糖组成
Analysis of polysaccharides in different yellow rice wine by pre-column derivatization and high performance capillary electrophoresis
摘要
Abstract
Used the 10 kinds of yellow rice wine samples produced by different manufacturers as test objects,the polysaccharide contents and its monosaccharide compositions were analyzed by anthrone sulfuric acid method and a 1-phenyl-3-methyl-5-pyrazolone (PMP) pre-column derivatization high performance capillary electrophoresis (HPCE) method,respectively.The results showed that the HPCE exhibited perfect isolation of the monosaccharides of the polysaccharide in the yellow rice wine.The contents and the monosaccharides of polysaccharide in the 10 kinds of yellow rice wine were obviously different.The polysaccharide contents of the sweet yellow rice wine among the ten samples ranged from 0.0361％ to 0.2412％,0.1457％ ～0.1463％ of semi sweet yellow rice wine and 0.0182％ ～0.1644％ of semi dry yellow rice wine.Among the 10 investigated samples,the polysaccharide contents were higher than that in the main health wine in the current markets.The main monosaccharide of the polysaccharide in the ten yellow rice wine samples were glucose as well as 17.833％ percents of fructose in "Tai hu zhi xing 1878",respective 1.64％ and 14.578％ percents of mannose in "He Jiu Wu Nian Chen" and "Shanghai Lao Jiu Ba Nian Chen".关键词
黄酒/多糖/柱前衍生/高效毛细管电泳Key words
yellow rice wine/polysaccharide/pre-column derivatization/high performance capillary electrophoresis (HPCE)分类
轻工纺织引用本文复制引用
陈传平,陈乃东,陈红风..柱前衍生-高效毛细管电泳法分析不同黄酒的多糖组成[J].食品工业科技,2018,39(8):221-225,5.基金项目
安徽省教育厅高校科学研究重点项目(KJ2015A361,KJ2012A277). （KJ2015A361,KJ2012A277）
