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芋头淀粉纳米颗粒的制备及其表征

彭晔 余振宇 郑志 姜绍通

食品工业科技2018,Vol.39Issue(9):6-10,5.
食品工业科技2018,Vol.39Issue(9):6-10,5.DOI:10.13386/j.issn1002-0306.2018.09.002

芋头淀粉纳米颗粒的制备及其表征

Preparation and characterization of taro starch nanoparticles

彭晔 1余振宇 1郑志 1姜绍通1

作者信息

  • 1. 合肥工业大学食品科学与工程学院,合肥工业大学农产品加工研究院,安徽省农产品精深加工重点实验室,安徽合肥230009
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摘要

Abstract

In this paper,taro starch as raw material treated by pullulanase debranching in different time,retrogradation at 4 ℃ was used to prepare starch nanoparticles.The structure and morphology of taro starch and starch nanoparticles were characterized by Zeta potentiometer,Fourier transform infrared spectroscopy,differential scanning calorimeter,X ray diffractometer and scanning electron microscope.The results showed that the average size of taro starch nanoparticles obtained by different enzymolysis time of(4,6,8 and 10 h) were 354.7,235.4,274.6 and 400.9 nm,respectively.Fourier infrared spectroscopy showed that there were no new characteristic peaks in taro starch nanoparticles,but the intermolecular force and hydrogen bonding were enhanced.Compared with the taro starch,the gelatinization temperature and enthalpy of the starch nanoparticles decreased,and the range of gelatinization temperature increased.The X-ray pattern changed from A-type to V-type,and the relative crystallinity decreased obviously.The taro starch nanoparticles were polygonal or spherical,the specific surface area increased,and there was a certain phenomenon of reunion.

关键词

芋头淀粉/酶解时间/纳米颗粒/性质

Key words

taro starch/enzymolysis time/nanoparticle/character

分类

轻工纺织

引用本文复制引用

彭晔,余振宇,郑志,姜绍通..芋头淀粉纳米颗粒的制备及其表征[J].食品工业科技,2018,39(9):6-10,5.

基金项目

安徽省科技攻关重大专项(16030701082). (16030701082)

食品工业科技

OA北大核心CSTPCD

1002-0306

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