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基于UHPLC-QTOF-MS的兰州百合植物化学成分鉴定

米璐 王珂雯 祝秀梅 王雪 杨曙明 廖小军 徐贞贞

食品工业科技2024,Vol.45Issue(2):48-58,11.
食品工业科技2024,Vol.45Issue(2):48-58,11.DOI:10.13386/j.issn1002-0306.2023030188

基于UHPLC-QTOF-MS的兰州百合植物化学成分鉴定

Identification of Phytochemical Components in Lilium davidiivar.unicolorusing UHPLC-QTOF-MS

米璐 1王珂雯 1祝秀梅 2王雪 3杨曙明 3廖小军 4徐贞贞1

作者信息

  • 1. 中国农业大学食品科学与营养工程学院,北京 100083||中国农业科学院农业质量标准与检测技术研究所,农业农村部农产品质量安全重点实验室,北京 100081
  • 2. 甘肃省农产品质量安全检验检测中心,甘肃兰州 730099
  • 3. 中国农业科学院农业质量标准与检测技术研究所,农业农村部农产品质量安全重点实验室,北京 100081
  • 4. 中国农业大学食品科学与营养工程学院,北京 100083
  • 折叠

摘要

Abstract

To explore the profiles of phytochemical components in geographical indication product of China Lilium davidii var.unicolor,the bulbs of which derived from five major producing areas of Gansu Province(Yuzhong County,Lanzhou City,Qilihe District,Lanzhou City,Lintao County,Dingxi City,Weiyuan County,Dingxi City,Yongjing County,Linxia City)were detected using ultra-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry(UHPLC-QTOF MS).Based on untargeted metabolomics technology,a total of 62 phytochemical components were putatively annotated in the bulbs of L.davidii var.unicolor.Among them,there were 22 kinds of amino acids,pept-ides and their derivatives(e.g.,glutathione),9 kinds of lipids and phospholipids(e.g.,lyso-phosphatidylcholin),7 kinds of saccharides(e.g.,rhamnose),7 kinds of phenolic acids(e.g.,ferulic acid and caffeic acid),4 kinds of flavonoids(e.g.,kaem-pferol),4 kinds of natural vitamins(e.g.,riboflavin and vitamin C),3 kinds of phenolamines(e.g.,feruloyl putrescine),2 kinds of coumarins(e.g.,gerberinside),2 kinds of alkaloids(e.g.,trigonelline),terpenoids(e.g.,abietic acid)and trite-rpenoid saponins(e.g.,eleutheroside E).The study would provide richer data and scientific evidence for the investigation and utilization of L.davidii var.unicolor.

关键词

兰州百合/植物化学成分/代谢组学/超高效液相色谱串联四极杆飞行时间质谱法(UHPLC-QTOF MS)/R语言

Key words

Lilium davidii var.unicolor/phytochemical components/metabolomics/ultra-high performance liquid chromatography-quadrupole time-of-flight mass spectrometry(UHPLC-QTOF MS)/R language

分类

轻工纺织

引用本文复制引用

米璐,王珂雯,祝秀梅,王雪,杨曙明,廖小军,徐贞贞..基于UHPLC-QTOF-MS的兰州百合植物化学成分鉴定[J].食品工业科技,2024,45(2):48-58,11.

基金项目

甘肃省农业农村厅项目(SDWJ2021-03) (SDWJ2021-03)

国家特色蔬菜产业技术体系(CARS-24-E) (CARS-24-E)

国家自然科学基金面上项目(32072234). (32072234)

食品工业科技

OA北大核心CSTPCD

1002-0306

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