Mg-9Gd-3.5Y-2Zn-0.5Zr合金材料喷丸强化工艺及摩擦磨损性能研究OA北大核心CSTPCD
Shot Peening Process and Friction and Wear Properties of Mg-9Gd-3.5Y-2Zn-0.5Zr Alloy
目的 提高Mg-9Gd-3.5Y-2Zn-0.5Zr合金的耐磨性能.方法 通过喷丸强化工艺对Mg-9Gd-3.5Y-2Zn-0.5Zr合金表面进行处理,在合金表面制备出纳米强化层,随后进行干滑动摩擦磨损试验,探究其喷丸强化后耐磨性能的改变.利用OM、SEM研究合金表层至内部晶粒尺寸及组织特征的变化.利用电子天平秤测量摩擦磨损试验前后质量的损失量.利用维氏显微硬度计测量合金强化层深度方向的硬度分布.利用SEM研究了合金摩擦磨损后的形貌特征,探究其磨损机制.结果 对Mg-9Gd-3.5Y-2Zn-0.5Zr合金进行表面喷丸处理后,表面分别出现了 200~370 μm厚的晶粒细化层,其中喷丸气压为0.4 MPa、时间为40s的试样的细晶强化层厚约为250 µm,硬度约为155HV,较原始试样提高了 50%左右.结论 经喷丸强化后,镁合金表面发生塑性变形,获得纳米晶.晶粒尺寸从表层到内部逐渐变大,呈现梯度变化,喷丸处理后试样磨损质量普遍降低,耐磨性能得到提高,其中气压为0.4 MPa、喷丸时间为40 s的试样的耐磨性最好.铸态试样的摩擦磨损中,磨粒磨损和黏着磨损发挥主要作用,喷丸强化工艺后,磨损机制发生改变,喷丸时间为60 s时,氧化磨损起主导作用.另外,随着喷丸气压的增大,疲劳磨损由辅助作用逐渐变为主导作用.
As an indispensable industrial structural element,magnesium plays a very important role.In current practical applications,compared with other alloys,magnesium alloy has a low density and a lighter structure,and has been applied in many fields such as automobiles,electronics,medical treatment,and military weapons.Rare earth magnesium alloys generally refer to magnesium alloys containing rare earth elements.The comprehensive mechanical properties of magnesium alloys can be further improved by adding zirconium,aluminum,zinc,rare earth and other elements to pure magnesium,combined with appropriate processing technology.Magnesium alloy is the lightest metal structural material in engineering applications,which has the advantages of high specific stiffness,high specific strength and easy recovery.However,magnesium alloys have the problem of poor wear resistance,which makes them fail in the wear process and shortens their service life,thus limiting the potential development of magnesium alloys.In order to overcome this problem,it is particularly important to study and improve the wear resistance of magnesium alloys.Shot peening is an important mechanical surface treatment technology,which can obtain nanocrystals by hardening or strengthening the surface,improve the wear resistance of materials,and is one of the effective ways to reduce the fatigue of parts and improve the life of parts.Compared with other mechanical surface treatment methods,the equipment is simple and low-cost and is not limited by the shape and position of the workpiece,with convenient operation.Secondly,the controllable plastic deformation can be effectively achieved by shot peening parameters. In this study,the surface of Mg-9Gd-3.5Y-2Zn-0.5Zr alloy was treated by shot peening process,and nano-strengthened layer was prepared on the surface of the alloy,and then dry sliding friction and wear experiments were carried out to explore the change of wear resistance of the alloy after shot peening.OM and SEM were used to study the changes of grain size and structure characteristics from the surface to the inside of the alloy,the mass loss before and after the friction and wear test was measured by electronic balance,the hardness distribution in the depth direction of the strengthened layer of the alloy was measured by Vickers microhardness tester,and the morphology characteristics of the alloy after friction and wear were studied by SEM,and the wear mechanism was explored. The results showed that after the surface peening of Mg-9Gd-3.5Y-2Zn-0.5Zr alloy,grain refining layers of about 200 to 370 μm appeared on the surface,in which the peening pressure was 0.4 MPa,the time was 40 s,the fine grain strengthening layer was about 250 μm,and the hardness was about 155HV.Compared with that of the original sample,the hardness was improved by about 50%,and the strengthening effect was the best.After shot peening,the surface of magnesium alloy has plastic deformation and nanocrystals are obtained.The grain size gradually increases from the surface to the inside,showing a gradient change.After shot peening,the wear quality of the sample is generally reduced,and the wear resistance is improved.The wear resistance of the sample is the best when the pressure is 0.4 MPa and the shot peening time is 40 s.In the friction-wear of as-cast samples,abrasive wear and adhesive wear play a major role.After the shot peening process,the wear mechanism changes.When the shot peening time is 60 s,the oxidation wear plays a leading role.In addition,with the increase of shot peening pressure,fatigue wear gradually changes from an auxiliary role to a leading role.
贺帅;张治民
中北大学材料科学与工程学院,太原 030051
机械工程
喷丸强化耐磨性能Mg-9Gd-3.5Y-2Zn-0.5Zr合金纳米晶
shot peeningwear resistanceMg-9Gd-3.5Y-2Zn-0.5Zr alloynanocrystalline
《表面技术》 2024 (007)
96-106 / 11
山西省关键核心技术和共性技术研发攻关专项(20201102019)Shanxi Province Key Core Technology and Common Technology R&D Special Project(20201102019)
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