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螺旋藻多酚复合纳米微胶囊的制备与稳定性分析

钟秋帆 李崴 孙玮鸿 李方巍 曾名湧

食品工业科技2024,Vol.45Issue(10):198-206,9.
食品工业科技2024,Vol.45Issue(10):198-206,9.DOI:10.13386/j.issn1002-0306.2023070075

螺旋藻多酚复合纳米微胶囊的制备与稳定性分析

Preparation and Stability Analysis of Spirulina Polyphenol Composite Nanocapsules

钟秋帆 1李崴 1孙玮鸿 1李方巍 1曾名湧1

作者信息

  • 1. 中国海洋大学三亚海洋研究院,海南三亚 527000||中国海洋大学食品科学与工程学院,山东青岛 266000
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摘要

Abstract

To improve the stability of Spirulina polyphenols through microencapsulation.Two types of microcapsules,Phe-PS and Phe-PS-Zein were prepared by embedding zein and porous starch(PS)in spirulina polyphenols(Phe).The microstructure,stability,antioxidant activity,and in vitro simulated digestion properties of Phe,Phe-PS,and Phe-PS-Zein were compared.The results showed that under the conditions of core to wall ratio of 1:10,temperature of 80℃,and magnetic stirring time of 120 minutes,the embedding rate of Phe-PS microcapsules was 60.29%.The encapsulation efficiency of Phe-PS-Zein microcapsules was the highest at core to wall ratio of 1:10,wall to material ratio of 1:1,stirring time of 90 minutes,temperature of 60℃,and pH of 7,reached 86.93%.The XRD and XPS spectra indicated that the diffraction peak intensity of the crystal decreased after the addition of zein,which was mainly related to the amorphous structure of zein.DSC analysis showed that the addition of protein as wall material improved the thermal stability of microcapsules.Compared with free Phe and Phe-PS,Phe-PS-Zein showed an increased ability to scavenge DPPH radicals and reduce Fe3+ by measuring its antioxidant activity,stability,and in vitro sustained-release effect.In summary,the Phe-PS-Zein particles could serve as an effective delivery carrier for Spirulina polyphenols.The results of this study would be expected to provide a theoretical and experimental basis for the high-value utilization of Phe.

关键词

螺旋藻多酚/多孔淀粉/玉米醇溶蛋白/微胶囊/结构表征/稳定性/抗氧化活性/体外消化

Key words

Spirulina polyphenols/porous starch/zein/microcapsule/structure characterization/stability/antioxidant activity/in vitro digestion

分类

农业科技

引用本文复制引用

钟秋帆,李崴,孙玮鸿,李方巍,曾名湧..螺旋藻多酚复合纳米微胶囊的制备与稳定性分析[J].食品工业科技,2024,45(10):198-206,9.

基金项目

海南省重点研发计划项目(ZDYF2021XDNY283). (ZDYF2021XDNY283)

食品工业科技

OA北大核心CSTPCD

1002-0306

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