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顶空固相微萃取-气相色谱-质谱联用技术结合电子舌分析不同残糖含量蓝莓酒体风味

王利萍 丁昱文 吴颜欣 邱树毅 戴怡凤 周鸿翔

食品与发酵工业2024,Vol.50Issue(11):294-300,7.
食品与发酵工业2024,Vol.50Issue(11):294-300,7.DOI:10.13995/j.cnki.11-1802/ts.038300

顶空固相微萃取-气相色谱-质谱联用技术结合电子舌分析不同残糖含量蓝莓酒体风味

Flavor analysis of blueberry wines with different residual sugar contents by headspace solid phase microextraction gas chromatography-mass spectrometry combined with electronic tongue

王利萍 1丁昱文 2吴颜欣 2邱树毅 1戴怡凤 3周鸿翔1

作者信息

  • 1. 贵州大学酿酒与食品工程学院,贵州省发酵工程与生物制药重点实验室,贵州贵阳,550025
  • 2. 贵州茅台(集团)生态农业产业发展有限公司,贵州丹寨,557500
  • 3. 贵州大学酿酒与食品工程学院,贵州省发酵工程与生物制药重点实验室,贵州贵阳,550025||北京食品营养与人类健康高精尖创新中心,北京工商大学,北京,100048
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摘要

Abstract

The flavor of blueberry wine affects its quality and sensory evaluation,so it is necessary to study the flavor compounds in blueberry wine.In this paper,the flavor of two semi-sweet blueberry wines and two semi-dry blueberry wines were investigated via head-space solid phase microextraction gas chromatography-mass spectrometry and electronic tongue.It was found that the bitterness and astrin-gency of the four blueberry wines showed a gradual increase with the decrease of residual sugar content,and there was no significant differ-ence in the sourness,post-bitterness,and post-astringency.Among the four blueberry wines,the semi-sweet blueberry wine contained higher levels of esters than the semi-dry blueberry wine,while the semi-dry blueberry wine contained higher levels of alcohol than the semi-sweet blueberry wine.Volatile flavor compounds,such as ethyl acetate,terpinolene,and ethyl dodecanoate were higher in semi-sweet blueberry wines,whereas compounds such as ethyl cinnamate,ethyl benzoate,and ethyl phenylacetate were higher in semi-dry blueberry wines,and l-octanol and acetic acid had no significant correlation with the degree of fermentation.In addition,partial least-squares discrimination analysis was used to identify 13 potential differential markers in the four blueberry wines,and combined with the odour active values study,it was found that meso-2,3-butanediol and linalool only contributed to the overall flavor of semi-sweet and semi-dry,respectively,whereas β-damascenone,2-phenylethanol,3-methyl-butanol,and acetic acid with odour active values>500 made a significant contribution to the overall flavor of the blueberry wines with different residual sugar contents.

关键词

发酵蓝莓酒/顶空固相微萃取-气相色谱-质谱联用技术/电子舌/偏最小二乘法判别分析/香气活度值

Key words

fermented blueberry wine/headspace solid phase microextraction gas chromatography-mass spectrometry/electronic tongue/partial least-squares discrimination analysis/odour active values

引用本文复制引用

王利萍,丁昱文,吴颜欣,邱树毅,戴怡凤,周鸿翔..顶空固相微萃取-气相色谱-质谱联用技术结合电子舌分析不同残糖含量蓝莓酒体风味[J].食品与发酵工业,2024,50(11):294-300,7.

基金项目

国家自然科学基金地区基金项目(32260640) (32260640)

蓝莓酒技术研发(黔科合支撑[2022]重点006号) (黔科合支撑[2022]重点006号)

国家自然科学基金青年科学基金项目(31801509) (31801509)

北京食品营养与人类健康高精尖创新中心开放基金项目(20182010) (20182010)

贵州省发酵工程与白酒酿造人才基地(黔人领发[2018]3号) (黔人领发[2018]3号)

科技平台及人才团队计划项目(黔科合平台人才(2018)5251) (黔科合平台人才(2018)

2022年贵州省高等学校教学内容和课程体系改革项目-酒类风味化学 ()

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