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HS-GC-MS联用测定河南传统西瓜豆酱中的挥发性成分

袁贵英 娄方慧 杨会会 刘宁波

现代食品科技2024,Vol.40Issue(7):219-226,8.
现代食品科技2024,Vol.40Issue(7):219-226,8.DOI:10.13982/j.mfst.1673-9078.2024.7.0799

HS-GC-MS联用测定河南传统西瓜豆酱中的挥发性成分

Analysis of the Volatile Components in Henan Traditional Watermelon Soybean Paste by HS-GC-MS

袁贵英 1娄方慧 1杨会会 1刘宁波2

作者信息

  • 1. 河南农业职业学院食品工程学院,河南郑州 451450
  • 2. 富鼎精密工业(郑州)有限公司,河南郑州 451450
  • 折叠

摘要

Abstract

Taking the traditional fermented watermelon soybean paste from Henan as the research object,the volatile components of the paste were analyzed by HS-GC-MS.The effects of equilibrium temperature,equilibrium time,vibration frequency and the amount of sodium chloride on the volatile compounds were investigated by single factor experiments.The results showed that the optimal conditions were as follows:equilibrium temperature,90℃;equilibrium time,50 min;vibration frequency,6 times per second;no sodium chloride added.Under these conditions,10 classes and 82 kinds of volatile compounds were identified in naturally fermented watermelon soybean paste,including 12 alcohols,10 esters,14 olefins,6 aldehydes,8 ketones,4 ethers,1 acid,10 alkanes,7 nitrogen-containing compounds and 10 other compounds.The relative contents of alkenes,aldehydes and alcohols were relatively high,accounting for 23.848%,22.537%and 19.743%,respectively.The sum of these three kinds accounted for 66.12%of the total volatile components,followed by esters and ketones(accounting for 11.945%and 6.839%,respectively).It can be concluded that the top three kinds of compounds play a vital role in the characteristic flavor of Henan traditional watermelon soybean paste.

关键词

自动顶空进样-气质联用/西瓜豆酱/挥发性成分

Key words

HS-GC-MS/watermelon soybean paste/volatile components

引用本文复制引用

袁贵英,娄方慧,杨会会,刘宁波..HS-GC-MS联用测定河南传统西瓜豆酱中的挥发性成分[J].现代食品科技,2024,40(7):219-226,8.

现代食品科技

OA北大核心CSTPCD

1673-9078

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