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花椒叶总黄酮超声辅助低共熔溶剂提取工艺优化及抗氧化性分析

孙伟 谷清义 翟冰倩 叶润 蔡静 乔新荣

食品与机械2025,Vol.41Issue(7):199-206,8.
食品与机械2025,Vol.41Issue(7):199-206,8.DOI:10.13652/j.spjx.1003.5788.2024.81115

花椒叶总黄酮超声辅助低共熔溶剂提取工艺优化及抗氧化性分析

Ultrasound-assisted extraction of total flavonoids from Zanthoxylum bungeanum Maxim.leaves with deep eutectic solvents and their antioxidant activity evaluation

孙伟 1谷清义 1翟冰倩 1叶润 1蔡静 1乔新荣1

作者信息

  • 1. 信阳农林学院药学院,河南 信阳 464000
  • 折叠

摘要

Abstract

[Objective]To investigate the effect of deep eutectic solvent(DES)on the extraction rate of total flavonoids from Zanthoxylum bungeanum Maxim.leaves and analyze their antioxidant activity.[Methods]Using Z.bungeanum leaves as raw material and total flavonoid extraction rate as the evaluation index,this study performs ultrasound-assisted extraction to screen the optimal DES system.The scavenging capacities of the extracted total flavonoids against hydroxyl radicals(·OH)and DPPH radicals are determined.[Results]The highest extraction rate of total flavonoids is achieved using a choline chloride-ethylene glycol DES system(ncholine chloride∶nethylene glycol=1∶3)with 22%water content,a solid-to-liquid ratio(mZ.bungeanum powder∶Vsolvent)of 1∶47(g/mL),and ultrasonic time of 15 min.The total flavonoids from Z.bungeanum leaves exhibit a maximum hydroxyl radical scavenging rate of(63.89±0.26)%and a DPPH radical scavenging rate as high as(89.01±0.51)%.[Conclusion]DES demonstrates excellent efficiency in extracting total flavonoids from Z.bungeanum leaves,and the extracted total flavonoids possess strong antioxidant activity.

关键词

低共熔溶剂/花椒叶/总黄酮/抗氧化

Key words

deep eutectic solvent/Zanthoxylum bungeanum Maxim.leaf/total flavonoids/antioxidant

引用本文复制引用

孙伟,谷清义,翟冰倩,叶润,蔡静,乔新荣..花椒叶总黄酮超声辅助低共熔溶剂提取工艺优化及抗氧化性分析[J].食品与机械,2025,41(7):199-206,8.

基金项目

河南省重点研发专项(编号:241111311400) (编号:241111311400)

信阳农林学院大别山道地中药资源与系列产品开发研究科技创新团队(编号:XNKJTD-009) (编号:XNKJTD-009)

河南省科技公关项目(编号:242102230094) (编号:242102230094)

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