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负载葡萄籽多酚油茶籽油纳米乳液的制备及表征

韩颖 刘佳保 李航 黄宗海 何新益 李云

食品与机械2025,Vol.41Issue(12):37-44,8.
食品与机械2025,Vol.41Issue(12):37-44,8.DOI:10.13652/j.spjx.1003.5788.2025.80645

负载葡萄籽多酚油茶籽油纳米乳液的制备及表征

Preparation and characterization of nanoemulsions of grape seed polyphenol-loaded camellia oil

韩颖 1刘佳保 1李航 1黄宗海 1何新益 1李云2

作者信息

  • 1. 天津农学院食品科学与生物工程学院,天津 300384
  • 2. 上饶师范学院生命科学学院,江西 上饶 334000||贵州布依丽吉油茶实业有限公司,贵州 黔西南州 562400
  • 折叠

摘要

Abstract

[Objective]To develop a highly stable camellia oil nanoemulsion system for loading grape seed polyphenol(GSP)to enhance its antioxidant property and solubility stability.[Methods]The formula is optimized based on the pseudo-ternary phase diagram method(moil phase∶msurfactant phase=8∶2,mTween 80∶mSpan 80=5∶5,absolute ethanol is used as the cosurfactant,and Km=4).The emulsion stability and water distribution are characterized by Zeta potential and low-field nuclear magnetic resonance,and its antioxidant activity is evaluated.[Results]The obtained W/O nanoemulsion has a particle size of(326.5±2.7)nm,an absolute value of Zeta potential of(46.4±0.2)mV,a polydispersity index(PDI)of 0.238,and an electrical conductivity of 4.8 μS/cm.When loaded with 1.5%GSP,the proportion of free water decreases to 17.21%,and the scavenging rates of DPPH free radicals and ABTS free radicals are 82.69%and 71.18%,respectively.After centrifugation(10 000 r/min),high temperature(90℃),low temperature(-4℃)and 30-day storage,there is no stratification,and the light transmittance is>95.8%.[Conclusion]This system combines high biological activity retention with long-lasting stability.

关键词

油茶籽油/纳米乳液/葡萄籽多酚/伪三元相图/抗氧化活性

Key words

camellia oil/nanoemulsion/grape seed polyphenol/pseudo-ternary phase diagram/antioxidant activity

引用本文复制引用

韩颖,刘佳保,李航,黄宗海,何新益,李云..负载葡萄籽多酚油茶籽油纳米乳液的制备及表征[J].食品与机械,2025,41(12):37-44,8.

基金项目

贵州省科技计划项目(编号:黔科合支撑[2023]一般483) (编号:黔科合支撑[2023]一般483)

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