无患子总皂苷质控品的制备OA北大核心CSCDCSTPCD
Preparation of total sapindus-saponins for quality control
无患子皂苷具有较好的洗涤功能,因其天然、安全、无毒,可开发成食品工业用清洗剂,而目前尚未有市售高纯度无患子总皂苷.以制备无患子总皂苷质控品为目标,通过乙醇提取、石油醚除杂、正丁醇萃取、AB-8大孔树脂、MCI凝胶柱分离纯化得无患子总皂苷,此无患子总皂苷再经液质联用(HPLC/MS)、Libermann-Buehard反应、溶血反应定性,香草醛-冰醋酸比色法定量.Libermann-Buehard反应颜色由黄-红-紫-蓝,有溶血性.HPLC/MS分…查看全部>>
Sapindus saponin has wonderful washing fuction which is natural,environment-frendly and nontoxic. It can be developed into food industry cleaning agent. However,there is no pure sapindus saponin commercially available. With the goal of producing the total sapindus saponin for quality control,the method of ethanol extraction,butanol extraction,AB-8 macroporous resin and MCI Gel column separation was used to separate and purify sapindus saponin. The qualitativ…查看全部>>
伍恒;张翠;翁震;徐德平;汪何雅;姚卫蓉
医药卫生
无患子皂苷齐墩果酸型三萜皂苷大孔树脂质量控制
sapindus saponinsoleanolic acid saponinsmacroporous resinquality control
《食品工业科技》 2013 (8)
91-96,6
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