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折光仪法在线检测盐酸和氢氧化钠溶液浓度的研究OACSTPCD

Online detection of concentration of hydrochloric acid and sodium hydroxide solutions by refractometer method

中文摘要英文摘要

建立准确测定盐酸溶液和氢氧化钠溶液浓度(以下简称酸液碱液浓度)的折光仪在线方法.通过分析pH计法和折光仪法检测酸液碱液浓度的影响因素,筛选出最佳检测方法-折光仪法;验证了折光仪法检测酸液碱液浓度的准确度、日内日间精密度,研究了旁管路安装与主管路角度变化、主管路的流速变化对检测效果的影响,及配置防爆清洗刷对检测效果的影响.结果表明:折光仪法检测结果更稳定,更适合用于酸液碱液浓度检测.检测结果与理论值绝对差值在 0.1%以内,日内日间精密度均<6%.以建立的酸液碱液浓度在线检测方法为手段,改进管路配置,结合流量计自动调整流速,实现了酸液碱液浓度的自动调配,且很好的将调配的酸液碱液浓度控制在0.7%~0.9%范围内.

Establish an online refractometer method for accurately measuring the concentration of hydrochloric acid solution and sodium hydroxide solution(hereinafter referred to as the concentration of acid and alkali solution).By analyzing the influencing factors of pH meter method and refractometer method to detect the concentration of acid and alkali solution,the best detection method-refractometer method was selected;Verified the accuracy and daytime precision of the refractometer method for detecting the concentration of acid and alkali solution.The impact of the installation of side pipelines and changes in the angle and flow rate of the main pipeline on the detection effect was studied,as well as the impact of configuring explosion-proof cleaning brushes on the detection effect.The results indicated that the refractometer method had more stable detection results and was more suitable for detecting the concentration of acid and alkali liquids.The absolute difference between the detection results and the theoretical value was within 0.1%,and the intra-day and inter-day precision was<6%.By using the established online detection method for acid and alkali concentration as a means,the pipeline configuration was improved,combining with the flow rate being automatically adjusted by a flow meter,the automatic allocation of acid and alkali concentration was achieved,and the concentration of the prepared acid and alkali was well controlled within the range of 0.7%to 0.9%.

吉桂珍;石文杰;周冬丽;张苹苹;杨啸;程远欣

河北晨光检测技术服务有限公司,邯郸 056107晨光生物科技集团股份有限公司,邯郸 057250

轻工业

折光仪在线氢氧化钠盐酸测定检测

refractometeronlinesodium hydroxidehydrochloric aciddeterminationdetection

《中国食品添加剂》 2024 (004)

284-288 / 5

10.19804/j.issn1006-2513.2024.4.034

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